Table 1 1H NMR and 13C NMR Spectroscopic Data for Compound 1.
From: Cytotoxic Rocaglate Derivatives from Leaves of Aglaia perviridis
Proton No. | 1 a | Proton No. | 1 a | ||
|---|---|---|---|---|---|
δH | δC | δH | δC | ||
1 | 5.11 d (6.5) | 79.8 | 3′5′ | 6.72 d (8.0) | 112.7 |
2 | 3.91 dd (14.0 7.0) | 50.5 | 4′ | 158.8 | |
3 | 4.32 d (14.5) | 55.0 | 1″ | 136.9 | |
3a | 102.0 | 2″6″ | 6.88 m | 127.9 | |
4a | 160.7 | 3″5″ | 7.11 m | 127.7 | |
5 | 6.46 d (2.0) | 93.4 | 4″ | 7.11 m | 126.6 |
6 | 159.7 | 1′′′ | 5.41 s | 93.7 | |
7 | 6.31 d (2.0) | 93.6 | 2′′′ | 4.67 s | 95.3 |
8 | 157.2 | 3′′′ | 4.25 t (7.5) 3.61 d (8.5) | 59.0 | |
8a | 110.0 | 4′′′ | 3.83 td (6.0, 2.0) | 68.6 | |
8b | 93.5 | 5′′′ | 4.24 td (11.0, 2.0) | 67.1 | |
8-OMe | 3.94 s | 56.0 | 6′′′ | 4.08 dd (11.0, 6.5) 3.99 dd (11.0, 6.5) | 64.1 |
4′-OMe | 3.77 s | 55.1 | COOCH3-2 | 3.67 s | 51.9 |
2′′′-OMe | 3.56 s | 55.1 | COOCH3-2 | 170.4 | |
1′ | 126.4 | 6′′′-CH3CO | 1.89 s | 20.5 | |
2′6′ | 7.15 d (8.0) | 129.1 | 6′′′-CH3CO | 171.0 | |
