Table 1 Identification of phenolic compounds in mulberry fruits by HPLC-DAD, LC-MS and LC-MS-MS.

From: Promotion of mitotic catastrophe via activation of PTEN by paclitaxel with supplement of mulberry water extract in bladder cancer cells

Peak No.

t R

Compound

λmax (nm)

[M + H]+/[M − H]−

MS-MS

Ref.

1

5.56

Quinic acid derivativec

233, 290

615/613

  

2

38.02

Neochlorogenic acidb

327, 244

/353

191(100), 179(86), 135(8)

Vallverdú – Queralt et al., 2012

3

38.88

Cyanidine 3-glucosidea

236, 282, 515

449

287(100), 426(16)

 

4

39.49

Cyanidine 3-rutinosidea

236, 282, 517

595

287(100), 449(52), 433(3)

 

5

40.92

Chlorogenic acida

328, 245

/353

191(100), 179(14), 173(1)

 

6

42.09

Cryptochlorogenic acidb

337, 245

/353

179(100), 173(95), 135(23)

Vallverdú – Queralt et al., 2012

7

48.53

Rutina

257, 233(sh), 357

/609

301(100), 300(67), 343(12)

 

8

49.24

Isoquercitrinb

257, 233(sh), 356

/463

301(100), 300(61), 343(3)

Yang et al., 2012

9

58.93

Phenolic derivativec

279, 234

/311

  

10

66.69

Phenolic derivativec

279, 236, 254

/279

  1. aThe identification was further confirmed by an authentic compound.
  2. bCompounds were tentatively identified according to mass spectra and matched data from the literature.
  3. cCompounds were limitedly identified from mass spectra and UV-visible absorbance spectra.