Table 1 The reflection table lists the crystallographic indices (hkl), the calculated phase of the structure factor (Φc), the measured phase obtained from the Kossel profile (Φm), their difference, the Laue/Bragg case and the source of the Kossel line.
From: Experimental phase determination of the structure factor from Kossel line profile
h k l | Φc (°) | Φm (°) | Φc–Φm (°) | L/B | source |
|---|---|---|---|---|---|
3 1 | 320.3 | 313.1 | 7.2 | L | As Kβ |
2 | 3.2 | 5.6 | −2.4 | L | As Kβ |
0 4 | 3.2 | −6.5 | 9.7 | L | As Kβ |
2 2 0 | 3.9 | 13.8 | −9.9 | L | As Kα1,2 |
| 47.2 | 47.5 | −0.3 | L | As Kα1,2 |
1 3 | 46.6 | 36.3 | 10.3 | L | As Kα1,2 |
| 46.6 | 37 | 9.6 | L | As Kα1,2 |
4 | 3.8 | −0.9 | 4.7 | L | As Kα1,2 |
1 | 321.6 | 315.5 | 6.1 | L | As Kα1,2 |
| 321.6 | 318.5 | 3.1 | L | As Kα1,2 |
| 321.8 | 311.9 | 9.9 | L | As Kα1,2 |
3 5 3 | 45.4 | 39.5 | 5.9 | L | As Kα1,2 |
2 2 0 | 3.9 | 13.6 | −9.7 | L | Ga Kβ |
| 317.2 | 313.5 | 3.7 | L | Ga Kβ |
| 316.6 | 310.4 | 6.2 | L | Ga Kβ |
4 | 3.8 | −6 | 9.8 | L | Ga Kβ |
2 2 0 | 1.3 | 15.2 | −13.9 | L | Ga Kα1,2 |
| 314.5 | 313.5 | 1 | L | Ga Kα1,2 |
3 3 1 | 314 | 312.4 | 1.6 | L | Ga Kα1,2 |
3 | 314 | 312.5 | 1.5 | L | Ga Kα1,2 |
2 2 | 1.3 | −17.5 | 18.8 | L | Ga Kα1,2 |
3 | 313.5 | 313.5 | 0 | L | Ga Kα1,2 |
| 313.1 | 304.4 | 8.7 | L | Ga Kα1,2 |
5 | 313.1 | 312.8 | 0.3 | L | Ga Kα1,2 |
| 49.4 | 57.1 | −7.7 | B | Ga Kα1,2 |
4 4 4 | 1.3 | 10.5 | −9.2 | B | Ga Kα1,2 |
3 1
3
2
5
3 5
3 1
3
2
3 1
3
3
1 5