Fig. 4: Electrochemical in situ FTIR spectra.

Electrochemical thin-layer in situ FTIR spectra of NO3−RR on Cu50Co50 (a), Cu (b), and Co (c) in 100 mM KNO3 + 1 M KOH. d \(\frac{{{{{{\rm{I}}}}}}_{{{{{{\rm{NO}}}}}}_{2}^{-}}}{{{{{{\rm{I}}}}}}_{{{{{{\rm{NH}}}}}}_{2}{{{{\rm{OH}}}}}}+{{{{{\rm{I}}}}}}_{{{{{{\rm{NO}}}}}}_{2}^{-}}}\) ratio at different electrode potentials. ATR-FTIR spectra on Cu50Co50 (e), Cu (f), and Co (g) in 1 M KOH.