Table. 1 List of screening experiments of different photocatalytic redox routes for amide synthesis
C-source | N-source | Product | Synthesis rate (μmol h−1)a |
|---|---|---|---|
CH3OH | NH3 | HCONH2 | 51.99 |
CH3OH | NO2− | HCONH2 | 40.44 |
CH3OH | NO3− | HCONH2 | 41.21 |
HCOOH | NH3 | HCONH2 | 0.32 |
HCOOH | NO2− | HCONH2 | trace |
HCOOH | NO3− | HCONH2 | 0.57 |
CH3CH2OH | NH3 | CH3CONH2 | 109.24 |
CH3CH2OH | NO2− | CH3CONH2 | 23.41 |
CH3CH2OH | NO3− | CH3CONH2 | 16.01 |
CH3COOH | NH3 | CH3CONH2 | trace |
CH3COONa | NH3 | CH3CONH2 | trace |
CH3COOH | NO2− | CH3CONH2 | 6.55 |
CH3COOH | NO3− | CH3CONH2 | trace |
