Table 2 Determination of lacidipine in mixtures with its degradation product by the proposed first derivative synchronous spectrofluorimetric procedure.
Intact (ng/ml) | Degradation product (ng/mL) | Degradation product (%) | Intact found (ng/mL) | %Recovery of intact |
---|---|---|---|---|
250 | 50 | 16.67 | 249.67 | 99.87 |
200 | 100 | 33.33 | 196.96 | 98.48 |
150 | 150 | 50 | 148.78 | 99.19 |
100 | 200 | 66.67 | 98.06 | 98.06 |
50 | 250 | 83.33 | 50.96 | 101.92 |
Mean ± %RSD | 99.50 ± 1.53 |