Table 1 Data collection and refinement statistics
|  | ∆14-PrfaH |
|---|---|
Data collection | |
Space group | P 43 |
Cell dimensions | Â |
a, b, c (Ã…) | 57.695, 57.695, 116.465 |
α, β, γ (°) | 90, 90, 90 |
Resolution (Å) | 32.21–2.0 (2.072–2.0)a |
Rsym or Rmerge | 0.06442 (0.5933) |
I/σI | 23.41 (4.30) |
Completeness (%) | 97.62 (92.66) |
Redundancy | 9.8 (8.1) |
Refinementb | |
Resolution (Ã…) | 2.0 |
No. of reflections | 25,084 (2359) |
Rwork/Rfree | 0.1728 (0.2102)/0.2123 (0.2785) |
No. of atoms | 2788 |
Protein | 2536 |
Ligand/ion | 7 |
Water | 245 |
B-factors | 38.61 |
Protein | 38.31 |
Ligand/ion | 48.83 |
Water | 41.41 |
R.m.s. deviations | Â |
Bond lengths (Ã…) | 0.003 |
Bond angles (°) | 0.57 |