Fig. 5: XRD pattern of Ba2.875PuO5.875 with profile refinement.
From: Structural and physical investigation of ordered BaO-deficient Ba3PuO6
Experimental (Yobs, in red) and calculated (Ycalc, in black) powder XRD patterns of Ba2.875PuO5.875 at ambient temperature. The sample is taken from the material obtained from synthesis 2 after 1323 K. Measurement at λ = Cu Kα1. The angular positions of Bragg reflections are shown in green. The difference between calculated and experimental intensities Yobs−Ycalc is shown in blue for the Rietveld refinement in space group I4/m. The uncertainties on optimised cell parameters and atomic positions are given in Tables 1 and 2.
