Table 1 Summary of the experimental conditions, crystal lattice parameters and the corresponding size of the GL nanoparticles.
From: Catechin tuned magnetism of Gd-doped orthovanadate through morphology as T1-T2 MRI contrast agents
Sample | Catechin molar ratio | Temperature (°C) | Duration (h) | Lattice parameters (Å) | Cell volume (Å3) | Crystallite size (nm) | Number mean diameter d (nm) | PDI |
|---|---|---|---|---|---|---|---|---|
MGL | 0 | 210 | 4 | a = 7.0168 Å; b = 7.2518 Å; c = 6.6957 Å | 329.31 | 8.82 | 798 | 0.59 |
TGL | 0.05 | 210 | 4 | a = b = 7.4306 Å; c = 6.5236 Å | 360.19 | 13.46 | 31.03 | 0.24 |
01GL | 0.01 | 180 | 24 | a = b = 7.4066 Å; c = 6.5088 Å | 357.06 | 6.84 | 68.99 | 0.33 |
5GL | 0.05 | 180 | 24 | a = b = 7.4464 Å; c = 6.5247 Å | 361.79 | 16.4 | 65.92 | 0.27 |
1GL | 0.1 | 180 | 24 | a = b = 7.4465 Å; c = 6.5321 Å | 362.21 | 13.32 | 32.57 | 0.27 |
