Table 2 Sample preparation and analytical techniques for the determination of mycotoxins in SEA fermented foods and raw materials used for preparing fermented foods.

From: The importance and mitigation of mycotoxins and plant toxins in Southeast Asian fermented foods

Commodity

Country

No of samples

Extraction Solvent

Clean -Up

Analytical method

Mycotoxins

Reference

Fermented Wine and Beer

Malaysia

10

Acetonitrile

SPE

LC-MS/MS

AF, OTA

Alsharif, et al.140

Thailand

200

Chloroform/Acetonitrile

DLME

LC-MS/MS

AF, ZEN, OTA, FB, T-2, DON

Puangkham, et al.141

Dried Chilli

Thailand

120

Methanol

*

TLC

AF, OTA

Chuaysrinule, et al.142

Indonesia

6

Methanol-Water

IAC

HPLC-UV

AF, OTA

Wikandari, et al.143

Malaysia

10

Acetonitrile

SPE

LC-MS/MS

AF, OTA

Alsharif, et al.140

Malaysia

80

Methanol-NaHCO3

IAC

HPLC-FL

AF, OTA

Jalili and Jinap144

Rice

Thailand

10

Methanol

SPE

LC-QTOFMS

AF, ZEN, OTA, FB, T-2, DON

Shiratori, et al.145

Vietnam

111

Methanol-Water

*

ELISA

AF, FB

Huong, et al.146

Thailand

240

Methanol

SPE

HPLC-FL

AF, FB

Panrapee, et al.147

Myanmar

21

Acetonitrile

SPE

LC-MS/MS

AF, FB

Lim, et al.148

Malaysia

50

Methanol

IAC

ELISA

AF, OTA

Lim, et al.148

Fish

Philippines

31

Ethanol

SPE

HPLC-UV

AF, OTA

Ebarvia, et al.149

Soybean (Tempeh)

Indonesia

9

Acetonitrile-Water

DnS

HPLC-MS/MS

ZEN

Borzekowski, et al.150

Palm Kernel Cake

Indonesia

20

Methanol-water

*

ELISA

AF

Reiter, et al.151

Malaysia

25

Acetonitrile-Water

*

LC-MS/MS

AF, ZEN, OTA, FB, T-2, DON

Yibadatihan, et al.152

Corn and Cornmeal

Vietnam

102

Methanol-Water

*

ELISA

AF, FB

Huong, et al.146

Thailand

55

Methanol

 

HPLC-UV

OTA

Singkong, et al.153

Indonesia

13

Methanol

BSA

ELISA

AF

Reiter, et al.151

Indonesia

16

Acetonitrile

IAC

HPLC-UV

AF, ZEN, OTA, FB, T-2, DON

Ali154

Philippines

50

Acetonitrile-Water

SPE

HPLC-FL

AF, ZEN, FB

Yamashita, et al.155

Thailand

27

Acetonitrile-Water

SPE

HPLC-FL

AF, ZEN, FB

Yamashita, et al.155

Indonesia

12

Acetonitrile-Water

SPE

HPLC-FL

AF, FB

Yamashita, et al.155

  1. AF aflatoxins, ZEN zearalenone, OTA ochratoxin, FB fumonisins, T-2 T-2 toxin, DON deoxynivalenol, ELISA enzyme linked enzyme linked immunosorbent assay, TLC thin layer chromatography, HPLC high performance liquid chromatography, FL fluorescence, UV ultraviolet, MS mass spectrometry, SPE solid phase extraction, DnS dilute and shoot, IAC immunoaffinity column, BSA bovine serum albumin, ND not detected.
  2. *Not stated or investigated.