Fig. 3: Structural evolution of the reaction between TMO811 oxide precursor and Li2O.
From: Unusual Li2O sublimation promotes single-crystal growth and sintering
a, In situ XRD characterization (λ = 0.182 Å) tracks the reaction between TMO811 oxide precursor and Li2O, following a procedure similar to that used for synthesizing NMC811 single crystals. b–g, Ex situ high-resolution TEM characterization of the reaction products between TMO811 oxide precursor and Li2O at critical temperatures indicated in a: at 300 °C (b), at 500 °C (c), at 500 °C after 7 h (d), at 750 °C (e), at 850 °C (f) and at 850 °C after 7 h (g).
