Table 1 Data collection statistics and refinement parameters for mTnfaip8.
From: The Tnfaip8-PE complex is a novel upstream effector in the anti-autophagic action of insulin
Tnfia8 (PDB code 5JXD) | |
|---|---|
Data collection | |
Space group | I222 |
Cell dimensions | |
a, b, c (Å) | 66.28, 71.57, 90.60 |
α, β, γ (°) | 90, 90, 90 |
Resolution (Å) | 33.14–2.03 (2.07–2.03)* |
R sym or R merge | 7.8 (86.9) |
Volume fraction of solvent (%) | 49.03 |
V m (Å3/Da) | 2.41 |
I / σI | 23.2 (1.6) |
Completeness (%) | 97.4 (74.8) |
Redundancy | 6.7 (4.8) |
Refinement | |
Resolution (Å) | 33.14–2.03 |
No. reflections | 13998 |
R work/R free | 0.237/0.287 |
No. atoms | |
Protein | 1519 |
Ligand/ion | 49 |
Water | 21 |
B-factors | |
Protein | 52.8 |
Ligand/ion | 66.1 |
Water | 43.0 |
R.m.s. deviations | |
Bond lengths (Å) | 0.008 |
Bond angles (°) | 1.54 |
Ramanchandran plot | |
Residues in favored regions (%) | 96.6 |
Residues in allowed regions (%) | 3.4 |
Residues in disallowed (%) | 0.0 |
