Table 1 Information of QSYQ samples.
No. | Group | Batch information of raw materials | Description | |||
|---|---|---|---|---|---|---|
HQ | DS | SQ | JX | |||
I1 | Intermediate | Lot 1 | Lot 1 | Lot 1 | /a | Intermediates produced using different batches of HQ, DS and SQ. |
I2 | Intermediate | Lot 2 | Lot 2 | Lot 2 | / | |
I3 | Intermediate | Lot 3 | Lot 3 | Lot 3 | / | |
I4 | Intermediate | Lot 4 | Lot 4 | Lot 4 | / | |
I5 | Intermediate | Lot 5 | Lot 5 | Lot 5 | / | |
I6 | Intermediate | Lot 1 | Lot 1b | Lot 1 | / | I6, I7 and I8 used identical raw materials with I1 but each group had one abnormal herb which was pre-extracted. |
I7 | Intermediate | Lot 1b | Lot 1 | Lot 1 | / | |
I8 | Intermediate | Lot 1 | Lot 1 | Lot 1b | / | |
I9 | Intermediate | Lot 1 | Lot 1 | Lot 1 | Lot 1 | I9, I10 and I11 used identical raw materials with I1 but three batches of JX were added respectively. |
I10 | Intermediate | Lot 1 | Lot 1 | Lot 1 | Lot 2 | |
I11 | Intermediate | Lot 1 | Lot 1 | Lot 1 | Lot 3 | |
P1 | Preparation | /c | Commercially available QSYQ pills whose batch numbers were 140601, 140711, 150110, 150312 and 150803, respectively. | |||
P2 | Preparation | |||||
P3 | Preparation | |||||
P4 | Preparation | |||||
P5 | Preparation | |||||
