Table 1 Precision test of HPLC method.
RRT/RPA | 1 | 2 | 3 | 4 | 5 | 6 | Mean | RSD% |
|---|---|---|---|---|---|---|---|---|
Peak 1 | 0.365 | 0.364 | 0.361 | 0.364 | 0.365 | 0.365 | 0.364 | 0.43 |
1.326 | 1.323 | 1.328 | 1.312 | 1.315 | 1.32 | 1.321 | 0.47 | |
Peak 2 | 0.432 | 0.432 | 0.428 | 0.431 | 0.432 | 0.432 | 0.431 | 0.37 |
0.74 | 0.751 | 0.743 | 0.744 | 0.742 | 0.742 | 0.744 | 0.51 | |
Peak 3 | 0.793 | 0.793 | 0.786 | 0.793 | 0.794 | 0.794 | 0.792 | 0.39 |
1.596 | 1.606 | 1.609 | 1.562 | 1.609 | 1.598 | 1.597 | 1.12 | |
Peak 4 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 |
1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | |
Peak 5 | 1.336 | 1.336 | 1.324 | 1.337 | 1.336 | 1.335 | 1.334 | 0.37 |
0.196 | 0.2 | 0.199 | 0.199 | 0.2 | 0.193 | 0.198 | 1.41 | |
Peak 6 | 1.956 | 1.957 | 1.941 | 1.957 | 1.956 | 1.956 | 1.954 | 0.32 |
0.111 | 0.113 | 0.115 | 0.111 | 0.112 | 0.114 | 0.113 | 1.41 | |
Peak 7 | 2.009 | 2.01 | 1.993 | 2.01 | 2.009 | 2.009 | 2.007 | 0.32 |
0.171 | 0.172 | 0.171 | 0.17 | 0.169 | 0.163 | 0.169 | 1.45 | |
Peak 8 | 2.051 | 2.052 | 2.035 | 2.053 | 2.051 | 2.052 | 2.049 | 0.33 |
0.602 | 0.61 | 0.609 | 0.597 | 0.6 | 0.601 | 0.603 | 1.93 | |
Peak 9 | 2.144 | 2.145 | 2.126 | 2.145 | 2.144 | 2.144 | 2.141 | 0.34 |
0.965 | 0.966 | 0.969 | 0.956 | 0.963 | 0.967 | 0.964 | 0.86 | |
Peak 10 | 1.257 | 1.257 | 1.246 | 1.258 | 1.264 | 1.25 | 1.255 | 0.35 |
0.019 | 0.02 | 0.02 | 0.019 | 0.019 | 0.019 | 0.019 | 0.47 | |
Peak 11 | 1.391 | 1.391 | 1.379 | 1.392 | 1.391 | 1.39 | 1.389 | 0.51 |
0.044 | 0.045 | 0.045 | 0.043 | 0.044 | 0.044 | 0.044 | 2.67 |