Table 1 Validation data for free MC-LR in porcine serum. *Absolute recovery expressed as extraction efficiency when spiked at 1.25 ng toxin per 250 µL serum, equating to 5 ng/mL.
Fortified Porcine Serum 5 ng/mL | |
|---|---|
Intra-day RSD (%) (n = 7) | 3.8 |
Inter-day RSD (%) (n = 20) | 3.8 |
Average conc. (repeatability) (ng/mL) | 5.2 |
Average conc. (reproducibility) (ng/mL) | 5.2 |
Absolute recovery (%)* | 85.1 |
CCα (ng/mL) | 0.03 |
CCβ (ng/mL) | 0.04 |