Figure 2 | Scientific Reports

Figure 2

From: Probing disorder in pyrochlore oxides using in situ synchrotron diffraction from levitated solids–A thermodynamic perspective

Figure 2The alternative text for this image may have been generated using AI.

(ad) Synchrotron X-ray diffraction images and the corresponding Rietveld structure refinement plots for the melt quench Gd2Zr2O7 at different temperatures. The inner pyrochlore ring (111) fades during heating at 673–1873K, completely disappears at 2573 K (ac), then reappears during cooling (d), confirming reversible order–disorder phase transformation.

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