Table 3 Experimental conditions and crystallographic data for Leucite and KAlSiO4-O1 plus corundum Nist 676a: samples at 3 and 15 h of synthesis run 3.
From: Synthesis and Characterization of Leucite Using a Diatomite Precursor
sample | 3 h, synthesis run 3 + 10% Corundum NIST 676a | 15 h, synthesis run 3 + 10% Corundum NIST 676a |
|---|---|---|
Wavelenght (Å) | 1.5418 | 1.5418 |
No. of observation | 2248 | 1589 |
R wp | 0.13 | 0.14 |
R p | 0.09 | 0.11 |
CHI 2 | 1.51 | 2.18 |
% amorphous | 5.40(11) | 0.11(8) |
% phase KAlSiO4-O1 | 15.95(14) | 0 |
% phase leucite | 78.65(15) | 99.89(18) |
Space group leucite | I41/a | I41/a |
a (Å) | 13.0712(51) | 13.0614(18) |
b (Å) | 13.0715(16) | 13.0671(38) |
c (Å) | 13.7511(17) | 13.7544(16) |
Space group KAlSiO4-O1 | P21 | / |
a (Å) | 15.6223(21) | / |
b (Å) | 9.0518(8) | / |
c (Å) | 8.5641(9) | / |
