Table 2 Quantities of reagents, isolated yields and run times from three semi-automated 211At isolation experiments.
NH2OH·HCl (mL) | 1.5 M HCl wash (mL) | H2O wash (mL) | % Isolation yield (decay-corrected) | Run time (min) | |
|---|---|---|---|---|---|
1 | 80 | 20 | 20 | 95.3 | 100 |
2 | 80 | 20 | 20 | 88a | 100 |
3 | 65 | 40 | 40 | 96.7 | 90 |