Table 2 X-ray data collection statistics of Hb1EmCO_hexa.
X-ray device | ELETTRA synchrotron | Rigaku FR007HF with CCD detector |
|---|---|---|
Space group | P 61 2 2 | P 61 2 2 |
Unit-cell parameters | ||
a, b, c (Å) | 91.70, 91.70, 168.72 | 91.63, 91.63, 169.12 |
α, β, γ (°) | 90.0, 90.0, 120.0 | 90.0, 90.0, 120.0 |
Asymmetric unit | αβ dimer | αβ dimer |
Data processing | ||
Resolution limits (Å) | 79.4–1.49 | 79.4–2.03 |
No. of reflections | 212199 | 86031 |
No. of unique reflections | 66710 | 25051 |
Completeness (%) | 96.4 (92.5) | 89.6 (65.2) |
I/σ (I) | 8.0 (2.1) | 24.7 (3.0) |
Average multiplicity | 3.2 (2.6) | 3.4 (2.6) |
Rmerge | 0.095 (0.440) | 0.071 (0.329) |
