Table 2 Comparison of matrix-matched calibration and solvent calibration at 10–1000 μg kg−1.
Compound | Matrix | Regression equation | R2 | Matrix effect (%) | LOD (μg kg−1) | LOQ (μg kg−1) |
|---|---|---|---|---|---|---|
Bifenthrin | n-Hexane | y = 917.43×−1669.74 | 0.9992 | — | — | — |
Oyster mushroom | y = 1378.65×+11014.79 | 0.9998 | 50.27 | 0.037 | 0.122 | |
Shiitake mushroom | y = 1406.06×+4712.20 | 0.9995 | 53.26 | 0.071 | 0.237 | |
Eryngii mushroom | y = 1410.36×−963.07 | 0.9992 | 53.73 | 0.021 | 0.069 | |
Crimini mushroom | y = 1350.62×+6803.68 | 0.9994 | 47.22 | 0.016 | 0.054 | |
Enoki mushroom | y = 1366.83 + 17846.90 | 0.9989 | 48.98 | 0.038 | 0.126 | |
Bunashimeji mushroom | y = 1419.98 + 5624.00 | 0.9999 | 54.78 | 0.025 | 0.083 | |
Fenpropathrin | n-Hexane | y = 69.32×−1602.22 | 0.9976 | — | — | — |
Oyster mushroom | y = 112.28×+156.06 | 0.9999 | 61.97 | 0.148 | 0.492 | |
Shiitake mushroom | y = 114.69×−108.54 | 0.9994 | 65.45 | 0.161 | 0.537 | |
Eryngii mushroom | y = 113.88×−558.57 | 0.9991 | 64.28 | 0.034 | 0.112 | |
Crimini mushroom | y = 107.86×+21.11 | 0.9995 | 55.60 | 0.105 | 0.351 | |
Enoki mushroom | y = 107.80×+871.59 | 0.9993 | 55.51 | 0.116 | 0.385 | |
Bunashimeji mushroom | y = 111.61×−255.32 | 0.9999 | 61.01 | 0.754 | 2.515 | |
Cyhalothrin | n-Hexane | y = 94.09×−2757.26 | 0.9952 | — | — | — |
Oyster mushroom | y = 185.33×−1579.27 | 0.9998 | 96.97 | 1.211 | 4.036 | |
Shiitake mushroom | y = 203.46×−1374.18 | 0.9990 | 116.24 | 0.304 | 1.014 | |
Eryngii mushroom | y = 195.85×−2845.42 | 0.9982 | 108.15 | 0.812 | 2.705 | |
Crimini mushroom | y = 178.54×−1265.32 | 0.9997 | 89.75 | 0.138 | 0.458 | |
Enoki mushroom | y = 181.44×−661.70 | 1.0000 | 92.84 | 0.230 | 0.767 | |
Bunashimeji mushroom | y = 176.70×−1785.85 | 0.9996 | 87.80 | 0.237 | 0.791 | |
Permethrin | n-Hexane | y = 229.92×−1715.55 | 0.9990 | — | — | — |
Oyster mushroom | y = 380.94×+9262.22 | 0.9992 | 65.68 | 0.059 | 0.196 | |
Shiitake mushroom | y = 398.28×+11871.62 | 0.9984 | 73.23 | 0.032 | 0.108 | |
Eryngii mushroom | y = 382.27×+2916.55 | 0.9993 | 66.26 | 0.026 | 0.086 | |
Crimini mushroom | y = 366.04×+8864.70 | 0.9991 | 59.20 | 0.015 | 0.051 | |
Enoki mushroom | y = 367.54×+8021.24 | 0.9989 | 59.86 | 0.036 | 0.119 | |
Bunashimeji mushroom | y = 384.23×+7303.04 | 0.9995 | 67.11 | 0.025 | 0.083 | |
Cyfluthrin | n-Hexane | y = 93.91×−2395.75 | 0.9985 | — | — | — |
Oyster mushroom | y = 234.30×−3149.71 | 0.9995 | 149.49 | 0.488 | 1.625 | |
Shiitake mushroom | y = 249.29×−2914.76 | 0.9987 | 165.46 | 1.163 | 3.876 | |
Eryngii mushroom | y = 230.07×−4354.54 | 0.9976 | 144.99 | 0.127 | 0.424 | |
Crimini mushroom | y = 212.24×−3468.49 | 0.9989 | 126.00 | 0.103 | 0.344 | |
Enoki mushroom | y = 205.24×−2701.42 | 0.9994 | 118.55 | 0.363 | 1.211 | |
Bunashimeji mushroom | y = 214.95×−3724.08 | 0.9983 | 128.89 | 1.073 | 3.576 | |
Cypermethrin | n-Hexane | y = 204.64×−7437.40 | 0.9936 | — | — | — |
Oyster mushroom | y = 475.19×+1202.65 | 0.9998 | 132.21 | 0.065 | 0.218 | |
Shiitake mushroom | y = 506.74×+13.76 | 0.9989 | 147.63 | 0.059 | 0.195 | |
Eryngii mushroom | y = 475.26×−1499.63 | 0.9983 | 132.24 | 0.126 | 0.419 | |
Crimini mushroom | y = 443.91×+2479.19 | 0.9993 | 116.92 | 1.259 | 4.198 | |
Enoki mushroom | y = 430.10×+1144.36 | 0.9998 | 110.17 | 0.723 | 2.411 | |
Bunashimeji mushroom | y = 451.72×+740.57 | 0.9989 | 120.74 | 1.221 | 4.068 | |
Flucythrinate | n-Hexane | y = 388.40×−12880.95 | 0.9945 | — | — | — |
Oyster mushroom | y = 1030.38×−7947.70 | 0.9999 | 165.29 | 0.451 | 1.503 | |
Shiitake mushroom | y = 1077.43×−8247.59 | 0.9991 | 177.40 | 0.222 | 0.739 | |
Eryngii mushroom | y = 1020.13×−9961.48 | 0.9988 | 162.65 | 0.869 | 2.896 | |
Crimini mushroom | y = 954.05×−8132.86 | 0.9995 | 145.64 | 0.070 | 0.233 | |
Enoki mushroom | y = 940.39×−3366.13 | 0.9999 | 142.12 | 0.149 | 0.496 | |
Bunashimeji mushroom | y = 970.90×−10710.4 | 0.9994 | 149.97 | 0.122 | 0.407 | |
Tau-fluvalinate | n-Hexane | y = 23.03×−268.86 | 0.9987 | — | — | — |
Oyster mushroom | y = 48.05×−1026.10 | 0.9964 | 108.64 | 0.468 | 1.560 | |
Shiitake mushroom | y = 54.90×−847.89 | 0.9961 | 138.38 | 0.355 | 1.183 | |
Eryngii mushroom | y = 49.10×−1231.91 | 0.9955 | 113.20 | 1.184 | 3.947 | |
Crimini mushroom | y = 43.50×−683.67 | 0.9969 | 88.88 | 0.604 | 2.015 | |
Enoki mushroom | y = 40.51×−732.66 | 0.9975 | 75.90 | 0.787 | 2.622 | |
Bunashimeji mushroom | y = 42.48×−867.74 | 0.9951 | 84.46 | 0.673 | 2.242 | |
Fenvalerate | n-Hexane | y = 116.97×−5266.69 | 0.9906 | — | — | — |
Oyster mushroom | y = 298.44×−5894.21 | 0.9991 | 155.14 | 0.669 | 2.229 | |
Shiitake mushroom | y = 319.06×−5407.40 | 0.9984 | 172.77 | 1.669 | 5.565 | |
Eryngii mushroom | y = 298.29×−6626.48 | 0.9975 | 155.01 | 1.374 | 4.580 | |
Crimini mushroom | y = 277.95×−5612.92 | 0.9987 | 137.63 | 1.048 | 3.492 | |
Enoki mushroom | y = 270.36×−4366.27 | 0.9995 | 131.14 | 0.750 | 2.499 | |
Bunashimeji mushroom | y = 277.19×−5915.89 | 0.9984 | 136.98 | 0.219 | 0.730 | |
Deltamethrin | n-Hexane | y = 31.82×−984.06 | 0.9953 | — | — | — |
Oyster mushroom | y = 86.78×−2872.02 | 0.9958 | 172.72 | 1.210 | 4.032 | |
Shiitake mushroom | y = 78.89×−2031.72 | 0.9967 | 147.93 | 0.071 | 0.238 | |
Eryngii mushroom | y = 85.89×−1656.28 | 0.9976 | 169.92 | 1.312 | 4.373 | |
Crimini mushroom | y = 75.92×−534.92 | 0.9962 | 138.59 | 0.035 | 0.118 | |
Enoki mushroom | y = 72.69×−1603.40 | 0.9953 | 128.44 | 0.076 | 0.252 | |
Bunashimeji mushroom | y = 70.21×−992.51 | 0.9989 | 120.65 | 0.093 | 0.310 |