Figure 4

Results of (a) FE-SEM observations and (b) XRD measurements of solid particles formed by various ratios of [reducing agents]/[CuO]. Hydrazine, sodium borohydride (NaBH4), and ascorbic acid (AA) were chosen as the reducing agents. (i) [N2H4]/[CuO]: 1.0; (ii) [N2H4]/[CuO]: 2.0; (iii) [N2H4]/[CuO]: 8.0; (iv) [N2H4]/[CuO]: 16; (v) [NaBH4]/[CuO]: 4.0; (vi) [AA]/[CuO]: 4.0;. The scale bar shown in (a)-(vi) is common for all images in (a).