Table 2 1H NMR and 13C NMR spectrum of compound A in acetone-d6.
No | 13C NMR | 1H NMR | No | 13C NMR | 1H NMR |
|---|---|---|---|---|---|
2 | 165.4 | 2" | 165.5 | 7.6 (d, J = 8 Hz) | |
3 | 101.8 | 6.54 (s) | 3" | 102.0 | 6.34 (s) |
4 | 182.1 | 4" | 182.2 | ||
5 | 162.0 | 5" | 160.0 | ||
6 | 98.7 | 6.04 (d, J = 2.0 Hz) | 6" | 101.8 | 6.31 (s) |
7 | 165.02 | 7" | 162.1 | ||
8 | 94.0 | 6.1 (d, J = 2.0 Hz) | 8" | 102.2 | |
9 | 158.0 | 9" | 155.5 | ||
10 | 102.2 | 10" | 108.0 | ||
1' | 120.0 | 1'" | 123.9 | ||
2' | 131.6 | 8.2 (d, J = 2.0 Hz) | 2'" | 127.9 | 7.67(d, J = 8.8 Hz) |
3' | 123.9 | 3'" | 114.0 | 6.44 (d, J = 8.8 Hz) | |
4' | 158.0 | 4"' | 162.1 | ||
5' | 120.0 | 7.04 (d, J = 8.7 Hz) | 5'" | 114.0 | 6.44 (d, J = 8.8 Hz) |
6' | 130.5 | 7.80 (dd, J = 2, 8.7 Hz) | 6'" | 127.86 | 7.67 (d, J = 8.8 Hz) |
4"'OCH3 | 54.7 | 3.65(s) |
