Table 3 Robustness results of the proposed HPLC method expressed as %RSD of the drug assay.
Condition | Caffeine | resveratrol | Raspberry Ketone | Octopamine | Synephrine | Hordenine | 2-phenethyl amine | |
|---|---|---|---|---|---|---|---|---|
Flow rate 0.9 mL/min | Flow rate 0.85 mL/min | 0.62 | 1.85 | 0.42 | 1.04 | 1.19 | 1.77 | 1.69 |
Flow rate 0.95 mL/min | 0.56 | 0.32 | 1.53 | 0.52 | 1.74 | 0.93 | 0.99 | |
Acetonitrile: 0.1% phosphoric acid 50:50,%v/v | Acetonitrile: 0.1% phosphoric acid 52:48,%v/v | 0.65 | 0.44 | 1.14 | 0.39 | 1.7 | 1.34 | 1.44 |
Acetonitrile: 0.1% phosphoric acid 48:52,%v/v | 0.2 | 1.14 | 0.29 | 0.35 | 1.25 | 0.41 | 0.56 | |