Table 5 Mean percentage recoveries of geosmin and 2-MIB from spiked raw water samples extracted using a hydrophilic C18 μSPE cartridge, 2-propanol elution solvent and GC–MS detection.

From: An automated micro solid phase extraction gas chromatography–mass spectrometry (μSPE-GC–MS) detection method for geosmin and 2-methylisoborneol in drinking water

Water type

Spiked concentration (ng L−1)

Geosmin

2-MIB

Recovery ± RSD (%)

Recovery ± RSD (%)

Oswestry reservoir

Blank

N.D.

N.D.

10

97.9 ± 3.8

96.3 ± 2.3

50

98.4 ± 4.4

96.12 ± 4.0

100

97.8 ± 2.6

98.2 ± 2.1

200

100.0 ± 2.6

96.0 ± 1.2

Huntington river

Blank

N.D.

N.D.

10

97.1 ± 2.4

96.6 ± 4.6

50

97.2 ± 3.0

95.1 ± 7.0

100

96.9 ± 1.8

95.8 ± 3.4

200

97.7 ± 1.9

96.7 ± 1.9

  1. N.D. not detected.