Table 6 Selected parameters and results obtained from the designed experiment.
Run | A | B | C | Step 1 | Step 2 | |||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
The average size of MFI zeolite grain (nm) | %Error | A | B | C | The average size of MFI zeolite crystals (nm | %Error | ||||||
Actual value | Predicted value | Actual value | Predicted value | |||||||||
1 | 48 | 0.6 | 8 | 409.55 | 409.67 | 0.03 | 24 | 165 | 0.15 | 298.36 | 297.35 | 0.3 |
2 | 34 | 0.1 | 4 | 355.67 | 355.42 | 0.07 | 13 | 172.5 | 0.15 | 210.36 | 209.55 | 0.4 |
3 | 34 | 0.6 | 12 | 270.86 | 271.11 | 0.09 | 2 | 172.5 | 0.05 | 190.75 | 188.36 | 1.2 |
4 | 48 | 0.1 | 8 | 622.2 | 622.58 | 0.06 | 13 | 165 | 0.25 | 200.85 | 200.71 | 0.07 |
5 | 34 | 0.6 | 4 | 410 | 410 | 0 | 13 | 172.5 | 0.15 | 210.56 | 209.55 | 0.5 |
6 | 34 | 0.35 | 8 | 550 | 552.60 | 0.5 | 13 | 180 | 0.05 | 120.42 | 120.53 | 0.09 |
7 | 34 | 0.35 | 8 | 558 | 552.60 | 1 | 13 | 180 | 0.25 | 206.97 | 207.08 | 0.05 |
8 | 20 | 0.1 | 8 | 97.45 | 97.33 | 0.1 | 24 | 180 | 0.15 | 145.53 | 144.27 | 0.9 |
9 | 34 | 0.35 | 8 | 562 | 552.60 | 1.7 | 2 | 165 | 0.15 | 210.48 | 213.22 | 1.3 |
10 | 34 | 0.35 | 8 | 545 | 552.60 | 1.4 | 13 | 172.5 | 0.15 | 203.56 | 209.55 | 2.8 |
11 | 20 | 0.6 | 8 | 318.2 | 317.82 | 0.05 | 13 | 172.5 | 0.15 | 210.56 | 209.55 | 0.5 |
12 | 48 | 0.35 | 12 | 344.9 | 344.52 | 0.1 | 13 | 172.5 | 0.15 | 213.6 | 209.55 | 1.9 |
13 | 34 | 0.1 | 12 | 318.1 | 318.10 | 0 | 24 | 172.5 | 0.25 | 198.22 | 199.58 | 0.7 |
14 | 20 | 0.35 | 4 | 123.7 | 124.08 | 0.3 | 2 | 180 | 0.15 | 180.86 | 183.35 | 1.3 |
15 | 34 | 0.35 | 8 | 548 | 552.60 | 0.8 | 13 | 165 | 0.05 | 310 | 309.86 | 0.04 |
16 | 48 | 0.35 | 4 | 574.65 | 574.53 | 0.02 | 2 | 172.5 | 0.25 | 210.6 | 208.21 | 1.1 |
17 | 20 | 0.35 | 12 | 177.75 | 177.87 | 0.07 | 24 | 172.5 | 0.05 | 240.67 | 242.03 | 0.64 |