Table 2 Accuracy and precision for the determination of the analyzed drugs in bulk form using the presented method.

From: In-lab synthesized turn-off fluorescence sensor for estimation of Gemigliptin and Rosuvastatin polypill appraised by Spider diagram, AGREE and whiteness metrics

Parameters

GEM

RSV

Nominal value (µg/mL)

0.2

1

2

0.1

0.5

1

Intra-day

 Found ± SD

0.199 ± 0.003

0.998 ± 0.012

2.028 ± 0.026

0.1006 ± 0.001

0.506 ± 0.004

0.991 ± 0.008

 Recovery%

99.50

99.80

101.40

100.60

101.20

99.10

 Er%

− 0.50

− 0.20

1.40

0.60

1.20

− 0.90

 RSD%

1.51

1.20

1.28

0.99

0.79

0.81

Inter-day

 Found ± SD

0.203 ± 0.002

1.009 ± 0.015

1.995 ± 0.025

0.1018 ± 0.001

0.504 ± 0.007

1.009 ± 0.009

 Recovery%

101.50

100.90

99.75

101.80

100.80

100.90

 Er%

1.50

0.90

− 0.25

1.80

0.80

0.90

 RSD%

0.99

1.49

1.25

0.98

1.39

0.89

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