Table 2 Designation of samples to experimental conditions and analytical techniques.
Storage temperature | Time point (weeks) | Analytical techniques |
|---|---|---|
Ambient (c.17 °C) | 0, 2, 4 | LC–IM–MS, TD–GC–MS |
− 20 °C | 2, 4 | LC–IM–MS, TD–GC–MS |
− 80 °C | 2, 4 | LC–IM–MS, TD–GC–MS |