Table 2 Synthesis of 2(a-l) by ChCl/HCA-DES.
Entry | Aldehyde | Product | Time (min) | Yield (%) | M.P. °C Found | M.P. °C literature | TON [a] | TOF [(b] |
|---|---|---|---|---|---|---|---|---|
1 |
| 2a | 25 | 90 | 155–165 | 160-16225 | 90 | 3.6 |
2 |
| 2b | 30 | 95 | 163–173 | 195-19725 | 95 | 3.16 |
3 |
| 2c | 35 | 83 | 270–276 | 268-27031 | 83 | 2.37 |
4 |
| 2d | 20 | 85 | 180–197 | 172-17425 | 85 | 4.25 |
5 |
| 2e | 25 | 95 | 199–220 | 242-24532 | 95 | 3.8 |
6 |
| 2f | 30 | 86 | 179–181 | 180-18227 | 86 | 2.86 |
7 |
| 2 g | 20 | 87 | 185–235 | 248-25033 | 87 | 4.35 |
8 |
| 2 h | 35 | 88 | 175–185 | NEW | 88 | 2.51 |
9 | 2i | 20 | 90 | 215–220 | 210-21234 | 90 | 4.5 | |
10 |
| 2j | 20 | 95 | 180–185 | 260-26235 | 95 | 4.75 |
11 |
| 2k | 15 | 96 | 281–283 | 285-28727 | 96 | 6.4 |
12 |
| 2 L | 20 | 95 | 160–167 | 170-17127 | 95 | 4.75 |











