Table 2 Accelerated stability study DS at 25 °C.
Time (days) | FA-Fluo | CGE-UV | IP-RPLC | |||||||
|---|---|---|---|---|---|---|---|---|---|---|
Fragments | Main peak | Dimer | Fragments | Main peak | Dimer | Main peak + dimer | Fragments | Main peak | Adducts | |
0 | 14% | 85% | 1% | 15% | 68% | 17% | 85% | 20% | 80% | 0% |
2 | 16% | 84% | 1% | 16% | 68% | 16% | 84% | 22% | 78% | 0% |
7 | 18% | 81% | 1% | 19% | 67% | 14% | 81% | 25% | 75% | 0% |
9 | 19% | 80% | 1% | 20% | 65% | 16% | 81% | 26% | 74% | 0% |
13 | 23% | 76% | 1% | 23% | 63% | 14% | 77% | 29% | 71% | 0% |
15 | 23% | 77% | 0% | 22% | 63% | 15% | 78% | 30% | 70% | 0% |
