Abstract
Sustainability concerns, environmental impact, and demand for renewable raw materials have intensified research efforts toward the development of novel natural fibres for textile applications. In this study, fibres extracted from the leaves of Agave fourcroydes were systematically investigated to evaluate their suitability as a sustainable textile fibre. Mature leaves were harvested and subjected to a water retting process followed by mechanical separation to extract the fibres, which were subsequently sun-dried. The extracted fibres were characterized for key textile-relevant properties including fibre length, bundle strength, fineness, colour characteristics, density, and thermal stability. In addition, morphological and chemical analyses were performed using scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR), respectively. The results indicate that Agave fourcroydes leaf fibres exhibit extra-long staple length, adequate bundle strength, and good thermal stability up to approximately 220 °C, making them suitable for common textile processing conditions. The overall performance of the fibres suggests that they can serve as a viable and eco-friendly alternative to conventional natural fibres, particularly for applications such as packaging textiles and similar functional textile products.
Data availability
The datasets generated during and/or analyzed during the current study are available from the corresponding author on reasonable request.
References
Egiza, M., Diab, M. R., Faisal, N. & Elsheikh, A. H. Natural fibers for enhanced efficiency and sustainability in solar desalination: A review. Solar Energy 282, 112963. https://doi.org/10.1016/j.solener.2024.112963 (2024).
Haidir, F. et al. Review: Natural fibres for textile application. IOP Conf. Ser. Earth Environ. Sci. 1358(1), 012006. https://doi.org/10.1088/1755-1315/1358/1/012006 (2024).
Akar, M. A., Tosun, A. T., Yel, F. & Kumlu, U. The usage of natural fibers for automotive applications. Macromol. Symp. https://doi.org/10.1002/masy.202100414 (2022).
Przybek, A. The role of natural fibers in the building industry—The perspective of sustainable development. Materials 18(16), 3803. https://doi.org/10.3390/ma18163803 (2025).
Sebastain, S. & Divya, P. V. Natural fibres: A sustainable material for geotextile applications. Indian Geotech. J. 54(3), 1056–1072. https://doi.org/10.1007/s40098-023-00862-w (2024).
Köktaş, S. et al. Extraction and Characterization of Natural Cellulosic Fibre from Taraxacum Sect. Ruderalia J. Nat. Fibres. 19, 14328–14336 (2022).
Indian standards specifications IS: 271, Textiles - Grading of White, Tossa and Daisee uncut Indian jute. Bureau of Indian Standards, New Delhi, 2003 and 2020.
Shinoj, S., Visvanathan, R., Panigrahi, S. & Kochubabu, M. Oil palm fibre (OPF) and its composites: A review. Ind. Crops Prod. 33 (1), 7–22 (2011).
Lakshmaiya, N. et al. Development of ecofriendly hybrid nanocomposites with improved antibacterial and mechanical properties through NaOH treated natural fibers. Results Eng. 26, 104996 (2025).
Sathishkumar, G. et al. Himadri Majumder, and Ashish Kumar Srivastava. Experimental study on mechanical performance and microstructural characterization of optimized sisal fiber reinforced polyester composites. Sci. Rep. 15 (1), 36348 (2025).
Bar, G. & Chaudhary, K. Characterization of textile grade novel Bauhinia Vahlii fibre. J. Nat. Fibres https://doi.org/10.1080/15440478.2022.2143464 (2022).
Sheferaw, L. et al. Extraction and characterization of fibre from the stem of cyperus papyrus plant. J. Nat. Fibres https://doi.org/10.1080/15440478.2022.2149661 (2022).
Wardiningsih, W. et al. Characterization of natural fibre extracted from Etlingera elatior stalk for textile applications. J. Nat. Fibres 19, 9384–9395 (2021).
Kanimozhi, M. & Vasugi, N. Characterization of Agave vera-cruz Mill leaf fibre for textile applications–An exploratory investigation. J. Nat. Fibres. 9, 219–228 (2012).
Pandey, R. et al. Tellicherry bark microfibre: Characterization and processing. J. Nat. Fibres 19, 13288–13299 (2022).
Mulyani, R. W. et al. Characterization of agro waste fibre extracted from the stem of Canna Edulis plant and its potential in the textiles. J. Nat. Fibres 19, 8909–8922 (2021).
Cazaurang-Martinez, M. N., Herrera-Franco, P. J. & Gonzalez-Chi, P. I. Physical and mechanical properties of Henequen fibres. J. Appl. Polym. Sci. 43, 749–756 (1991).
Han, S. O., Ahn, H. J. & Cho, D. Hygrothermal effect on Henequen or silk fibre reinforced poly(butylene succinate) biocomposites. Compos. Part B Eng. 41, 491–497 (2010).
Yasin, P. et al. A study of continuous Henequen/Epoxy composites. Mater. Today Proc. 18, 3798–3811 (2019).
Herrera-Franco, P. J. & Valadez-González, A. A study of the mechanical properties of short natural-fibre reinforced composites. Compos. Part B Eng. 36, 597–608 (2005).
Valadez-Gonzalez, A., Cervantes-Uc, J. M. & Olayo, R. Chemical modification of Henequén fibres with an organosilane coupling agent. Compos. Part B Eng. 30, 321–331 (1999).
Espinach, F. X., Julian, F. & Alcalà, M. Effective tensile strength estimation of natural fibres through micromechanical models: The case of Henequen fibre reinforced-PP composites. Polymers 14, 4890 (2022).
Kim, J. & Cho, D. Effects of alkali-treatment and feeding route of Henequen fibre on the heat deflection temperature, mechanical, and impact properties of novel Henequen fibre/Polyamide 6 composites. J. Compos. Sci. 6, 89 (2022).
Luo, S. & Netravali, A. N. Characterization of Henequen fibres and the Henequen fibre/poly(hydroxybutyrate-co-hydroxyvalerate) interface. J. Adhes. Sci. Technol. 15, 423–437 (2001).
Choi, H. Y., Han, S. O. & Lee, J. S. The effects of morphological properties of Henequen fibre irradiated by EB on the mechanical and thermal properties of Henequen fibre/PP composites. Compos. Interfaces 16, 751–768 (2009).
Gonzalez-Murillo, C. & Ansell, M. P. Mechanical properties of Henequen fibre/Epoxy resin composites. Mech. Compos. Mater. 45, 435–442 (2009).
Madival, A. S. et al. Processing, characterization of Furcraea foetida (FF) fibre and investigation of physical/mechanical properties of FF/epoxy composite. Polym 14, 1476 (2022).
Baskaran, P. G., Kathiresan, M. & Pandiarajan, P. Effect of alkali-treatment on structural, thermal, tensile properties of Dichrostachys cinerea bark fibre and its composites. J Nat Fibres 19, 433–49 (2020).
Pathan, Y. & Gb, V. K. Potential of Agave angustifolia marginata for composite and textile applications – A new source of natural fibre. Ind. Crops Prod. 203, 117213 (2023).
Samanta, R. et al. A comparative study on various natural plant fiber composites. J. Inst. Eng. (India): Ser. D, 106, 1–10 (2024).
Lee, C. H. et al. A comprehensive review on bast fibre retting process for optimal performance in fibre-reinforced polymer composites. Adv. Mater. Sci. Eng. 2020, 1–27 (2020).
Li, Y. & Shen, Y. O. The use of sisal and henequen fibres as reinforcements in composites. In Biofibre Reinforcements in Composite Materials, 165–210 (Elsevier, 2015).
Indran, S., Divya, D., Raja, S., Sanjay, M. R. & Siengchin, S. Physico-chemical, mechanical and morphological characterization of Furcraea selloa K. Koch plant leaf fibres-an exploratory investigation. J. Nat. Fibres https://doi.org/10.1080/15440478.2022.2146829 (2022).
Hulle, A., Kadole, P. & Katkar, P. Agave americana leaf fibres. Fibres 3, 64–75 (2015).
Banik, S. et al. Ribbon retting of jute—a prospective and eco-friendly method for improvement of fibre quality. Ind. Crops Prod. 17, 183–190 (2003).
Yasin, P., Venkataramana, M. & Kudari, S. K. Physio-mechanical properties and thermal analysis of Furcreo Foetedo Mediopicta (ffm) Fibres: Its potential application as reinforcement in making of composites. Learn. Anal. Intell. Syst. 492–500 (2019).
Sari, N. H., Wardana, I. N. G., Irawan, Y. S. & Siswanto, E. Characterization of the chemical, physical, and mechanical properties of NaOH-treated natural cellulosic fibres from corn husks. J. Nat. Fibres 15(4), 545–558 (2017).
Kommula, V. P. et al. Extraction, modification, and characterization of natural lignocellulosic fibre strands from Napier grass. Int. J. Polym. Anal. Charact. 21(1), 18–28 (2016).
Balaji, A. N., Karthikeyan, M. K. V. & Vignesh, V. Characterization of new natural cellulosic fibre from Kusha grass. Int. J.Polym. Anal. Charact 21, 29–39 (2016).
Fan, M., Dai, D. & Huang, B. Fourier transform infrared spectroscopy for natural fibres. Fourier Transform - Mater. Anal. https://doi.org/10.5772/35482 (2012).
Sanjay, M. R., Madhu, P. & Jawaid, M. Characterization and properties of natural fibre polymer composites: A comprehensive review. J. Clean. Prod. 172, 566–581 (2018).
Santhanam, K., Kumaravel, A. & Saravanakumar, S. S. Characterization of new natural cellulosic fibre from the *Ipomoea staphylina* plant. Int. J. Polym. Anal. Charact. 21, 267–274 (2016).
Zhuang, J. et al. Observation of potential contaminants in processed biomass using fourier transform infrared spectroscopy. Appl. Sci. 10, 4345 (2020).
Zhang, X. et al. Effect of steam pressure on chemical and structural properties of kenaf fibres during steam explosion process. BioResources https://doi.org/10.15376/biores.11.3.6590-6599 (2016).
Madhu, P., Sanjay, M. R. & Jawaid, M. A new study on effect of various chemical treatments on *Agave americana* fibre for composite reinforcement: Physico-chemical, thermal, mechanical and morphological properties. Polym. Test. 85, 106437 (2020).
El Ghali, A., Ben Marzoug, I. & Baouab Mhv, E. A. Separation and characterization of new cellulosic fibres from the Juncus acutus L plant. Bioresources https://doi.org/10.15376/Biores.7.2.2002-2018 (2012).
Sain, M. & Panthapulakkal, S. Bioprocess preparation of wheat straw fibres and their characterization. Ind. Crops Prod. 23, 1–8 (2006).
NagarajaGanesh, B. & Muralikannan, R. Extraction and characterization of lignocellulosic fibres from Luffa cylindrica fruit. Int. J. Polym. Anal. Charact. 21, 259–266 (2016).
Boopathi, L., Sampath, P. S. & Mylsamy, K. Investigation of physical, chemical and mechanical properties of raw and alkali treated Borassus fruit fibre. Compos. Part B Eng. 43, 3044–3052 (2012).
Dubey, S. C., Patil, S., Mishra, V. & Sharma, A. Agricultural waste fiber/filler composites: a review on physical, mechanical and wear behaviour. Discover Appl. Sci. 8 (1), 10 (2025).
Lakshmaiya, N. et al. Experimental evaluation of mechanical, fatigue, and tribological properties of kenaf fiber–epoxy composites reinforced with silicon carbide. Discover Appl. Sci. 7 (11), 1233 (2025).
Saha, S. C., Sarkar, A., Sardar, G., Ray, D. P. & Roy, G. Grading system of ramie fibre. Int. J. Bioresour. Sci. 4(1), 9–12 (2017).
Reddy, N. & Yang, Y. Preparation and characterization of long natural cellulose fibres from wheat straw. J. Agric. Food Chem. 55 (21), 8570–8575 (2007).
Binoj, J. S., Edwin Raj, R. & Sreenivasan, V. S. Morphological, physical, mechanical, chemical and thermal characterization of sustainable Indian Areca fruit husk fibres (Areca Catechu L.) as potential alternate for hazardous synthetic fibres. J. Bionic Eng. 13, 156–165 (2016).
Jeyapragash, R., Srinivasan, V. & Sathiyamurthy, S. Mechanical properties of natural fibre/particulate reinforced epoxy composites – A review of the literature. Mater. Today Proc. 22, 1223–1227 (2020).
Sahayaraj, A. F. Extraction and characterization of sponge gourd outer skin fibre. J. Nat. Fibres https://doi.org/10.1080/15440478.2023.2208888 (2023).
Pandey, R., Jose, S. & Sinha, M. K. Fibre extraction and characterization from Typha domingensis. J. Nat. Fibres 19, 2648–2659 (2020).
Chokshi, S., Gohil, P. & Lalakiya, A. Tensile strength prediction of natural fibre and natural fibre yarn: Strain rate variation upshot. Mater. Today Proc. 27, 1218–1223 (2020).
Nijandhan, K. & Muralikannan, R. S. K. Extraction and characterization of novel natural cellulosic fibres from pigeon pea plant. J. Nat. Fibres 17, 769–779 (2018).
Balasundar, P. et al. Extraction and characterization of new natural cellulosic Chloris barbata fibre. J. Nat. Fibres 15, 436–444 (2017).
Gaye, A. et al. Extraction and physicomechanical characterisation of *Typha australis* fibres: Sensitivity to a location in the plant. J. Nat. Fibers https://doi.org/10.1080/15440478.2022.2164106 (2023).
Rao, K. M. M. & Rao, K. M. Extraction and tensile properties of natural fibres: Vakka, date and bamboo. Compos. Struct. 77, 288–295 (2007).
Gopi Krishna, M., Kailasanathan, C. & NagarajaGanesh, B. Physico-chemical and morphological characterization of cellulose fibres extracted from *Sansevieria roxburghiana* Schult. & Schult. F leaves. J. Nat. Fibres. 19, 3300–3316 (2020).
Alzarieni, K. Z. et al. Characterization of Natural cellulosic fibre obtained from the flower heads of milk thistle (Silybum marianum) as a potential polymer reinforcement material. J. Nat. Fibres https://doi.org/10.1080/15440478.2023.2211289 (2023).
Pathan, Y. & Kumar, G. B. V. Studies on betterutilization of jute (Corchorus olitorius) plants harvested for seeds in South India-development of a novelmethod and machine: Part-I. Indian J. Agric. Res. https://doi.org/10.18805/ijare.a-6081 (2023).
Rana, M. N. et al. Properties of low-density cement-bonded composite panels manufactured from polystyrene and jute stick particles. J. Wood Sci. https://doi.org/10.1186/s10086-019-1831-3 (2019).
Banik, S., Basak, M. K. & sil, S. C. Effect of inoculation of pectinolytic mixed bacterial culture on improvement of ribbon retting of jute and kenaf. J. Nat. Fibres. 4, 33–50 (2007).
Matusiak, M. & Frydrych, I. Investigation of naturally coloured cotton of different origin–Analysis of fibre properties. Fibres Text. East. Eur. 5(107), 34–42 (2014).
Święch, T. & Frydrych, I. Naturally coloured cottons: Properties of fibres and yarns. Fibres Text. East. Eur. 7(4), 25–29 (1999).
Basu, G., Roy, A. N., Satapathy, K. K., Sk Md, J. & Abbas, L. M. and R. Chakraborty. Potentiality for Value-Added technical use of Indian sisal. Ind. Crops Prod. 36, 33–40.
Das, P. K., Nag, D., Debnath, S. & Nayak, L. K. Machinery for extraction and traditional spinning of plant fibres. Indian J. Tradit. Knowl. 9(2), 386–393 (2010).
Roy, S. & Lutfar, L. B. Bast fibres. In Elsevier eBooks, 39–59 (2012). https://doi.org/10.1016/b978-0-12-818398-4.00003-7
Saville, B. Fibre dimensions. In Elsevier eBooks, 44–76 (1999). https://doi.org/10.1533/9781845690151.44
Kiron, M. I. Torsional properties of fiber and textile materials. Textile Learner. (2022). https://textilelearner.net/torsional-properties-of-textile-fiber/?utm_source
Shuvo, I. I. Fibre attributes and mapping the cultivar influence of different industrial cellulosic crops (cotton, hemp, flax, and canola) on textile properties. Bioresources and Bioprocessing https://doi.org/10.1186/s40643-020-00339-1 (2020).
Atav, R., Yüksel, M. F., Dilden, D. B. & İzer, G. Colored cotton fabric production without dyeing within the sustainablity concept in textile. Ind. Crops Prod. 187, 115419. https://doi.org/10.1016/j.indcrop.2022.115419 (2022).
Kumar, M., Singh, V. P., Bhat, S. B. & Kumar, R. Environmental risks of textile dyes and photocatalytic materials for sustainable treatment: Current status and future directions. Discover Environ. https://doi.org/10.1007/s44274-025-00337-0 (2025).
Durand, V. The challenges around the fastness of natural dyes for textiles. Open Access Gov. 48(1), 458–459. https://doi.org/10.56367/oag-048-11634 (2025).
Balakrishnan, S., Wickramasinghe, G. D. & Wijayapala, U. S. A novel approach for banana (Musa) pseudo-stem fibre grading method: Extracted fibres from Sri Lankan banana cultivars. J. Eng. Fibres Fabr. 15, 1–9 (2020).
Basu, G. & Roy, A. N. Blending of jute with different natural fibres. J. Nat. Fibres 4, 13–29 (2008).
Sarkar, S. & Jha, A. K. Research for sisal (Agave sp.) fibre production in India. Int. J. Curr. Res. 9(11), 61136–61146 (2017).
Jasti, A. & Biswas, S. Characterization of elementary industrial hemp (Cannabis sativa L.) fibre and its fabric. J. Nat. Fibres https://doi.org/10.1080/15440478.2022.2158982 (2023).
Alwani, M. S. et al. An Approach to using agricultural waste fibres in biocomposites application: Thermogravimetric analysis and activation energy study. BioResources https://doi.org/10.15376/biores.9.1.218-230 (2013).
Legrand, N. B. R., Lucien, M. & Pierre, O. Physico-chemical and thermal characterization of a lignocellulosic fibre, extracted from the bast of Cola lepidota stem. J. Miner. Mater. Charact. Eng. 08, 377–392 (2020).
Belouadah, Z., Ati, A. & Rokbi, M. Characterization of new natural cellulosic fibre from Lygeum spartum L. Carbohydr. Polym. 134, 429–437 (2015).
Maheshwaran, M. V. et al. Characterization of natural cellulosic fibre from Epipremnum aureum stem. J. Nat. Fibres. 15, 789–798 (2017).
Venkatesha, P. G., Sai Abhi Chandan, V. & Sri Harsha, A. V. N. Chemical treatment and fibre length, their effect on the mechanical properties of blended composites. Mater. Today Proc. 44, 4862–4866 (2021).
Suresh, A., Bhargavi, P. & Kiran Kumar, M. Simulation and mechanical characterization on Kevlar epoxy reinforced composite with silicon carbide filler. Mater. Today Proc. 38, 2988–2995 (2021).
Venkatesha Prasanna, G., Neeraj Kumar, J. & Akhil Kumar, K. Optimisation & mechanical testing of hybrid biocomposites. Mater. Today Proc. 18, 3849–3855 (2019).
Brebu, M. & Vasile, C. Thermal degradation of lignin – A review. Cellul. Chem. Technol. 44(9), 353–363 (2010).
Selvaraj, M. & Mylsamy, S. A. B. Characterization of new natural fibre from the stem of Tithonia diversifolia plant. J. Nat. Fibres https://doi.org/10.1080/15440478.2023.2167144 (2023).
Selvaraj, M. Extraction and characterization of a new natural cellulosic fibre from bark of Ficus carica plant as potential reinforcement for polymer composites. J. Nat. Fibres https://doi.org/10.1080/15440478.2023.2194699 (2023).
Manivel, S. et al. Physico-mechanical, chemical composition and thermal properties of cellulose fibre from Hibiscus vitifolius plant stalk for polymer composites. J. Nat. Fibres 19, 6961–6976 (2021).
Selvaraj, M., Chapagain, P. & Mylsamy, B. Characterization studies on new natural cellulosic fibre extracted from the stem of Ageratina adenophora plant. J. Nat. Fibres https://doi.org/10.1080/15440478.2022.2156019 (2022).
Gopinath, R., Billigraham, P. & Sathishkumar, T. P. Physicochemical and thermal properties of cellulosic fibre extracted from the bark of *Albizia saman*. J. Nat. Fibers. 19, 6659–6675 (2021).
Indran, S. & Raj, R. E. Characterization of new natural cellulosic fibre from *Cissus quadrangularis* stem. Carbohydr. Polym. 117, 392–399 (2015).
Manimaran, P. et al. Physico-chemical properties of fibre extracted from the flower of Celosia argentea plant. J. Nat. Fibres 18, 464–473 (2019).
Bhuvaneshwaran, M. et al. Natural cellulosic fibre from Coccinia indica stem for polymer composites: Extraction and characterization. J. Nat. Fibres 18, 644–652 (2019).
Senthamaraikannan, P. et al. Characterization of natural cellulosic fibre from bark of Albizia amara. J. Nat. Fibres. 16, 1124–1131 (2018).
Amutha, V. & Senthilkumar, B. Physical, chemical, thermal, and surface morphological properties of the bark fibre extracted from *Acacia concinna* plant. J. Nat. Fibers. 18, 1661–1674 (2019).
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Yasin Pathan: Writing—Original Draft; Nikhil Alapakam: Investigation; Hemavathy R V: Conceptualization; K. Vijetha: Writing—Review & Editing; Subbarama Kousik Suraparaju: Project administration; Ramu Karthik: Formal analysis; V Krishna Kanth: Methodology; Pawan Kumar Singotia: Writing—Review & Editing; Anurag Joshi: Supervision.
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Pathan, Y., Alapakam, N., Hemavathy, R.V. et al. Extraction of natural fibres from Agave fourcroydes leaves and multi-property evaluation for potential textile applications. Sci Rep (2026). https://doi.org/10.1038/s41598-026-42567-z
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DOI: https://doi.org/10.1038/s41598-026-42567-z