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Synthesis and multi-technique structural characterization of trimetallic oxide nanocomposites for environmental and medicinal applications
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  • Published: 30 April 2026

Synthesis and multi-technique structural characterization of trimetallic oxide nanocomposites for environmental and medicinal applications

  • Sadaf Ilyas Awan1,
  • Wajid Rehman1,
  • Rida Zameer1,
  • Mona A. Alamri2,
  • Thoraya A. Farghaly3,
  • Muhammed Shakeel4,
  • Abdullah Y. A. Alzahrani5 &
  • …
  • Farrukh Khan6 

Scientific Reports (2026) Cite this article

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Subjects

  • Chemistry
  • Materials science
  • Nanoscience and technology

Abstract

This study aimed to synthesize a trimetallic oxide nanocomposite (NC) consisting of copper oxide (CuO), tin dioxide (SnO2) and hematite (Fe2O3) employing a sol-gel technique. Subsequently, the synthesized nanocomposite was calcined in an oxygen-rich environment at 100, 300, 600, and 900 °C. In order to investigate the morphological, optical, as well as structural characteristics of resulting nanocomposites, fourier transform infrared (FT-IR) spectroscopy, thermo-gravimetric analysis (TGA), scanning electron microscopy (SEM), X-ray diffraction (XRD), energy dispersive X-ray (EDX) spectroscopy, and ultraviolet–visible (UV-Vis) spectroscopy were employed. As demonstrated by variations in SEM micrographs, FT-IR bands, and XRD diffraction patterns, these investigations confirmed the successful synthesis of the nanocomposites and emphasized the significant impact of calcination temperature on their morphological and structural characteristics. For the degradation of crystal violet (CV) dye, synthesized nanocomposites were further analyzed as photocatalysts where the sample calcined at 100 °C exhibited the highest degradation efficiency i.e., 90.95%. In addition, significant biological activity was shown by these nanocomposites demonstrating promising antioxidant as well as antibacterial characteristics, thereby revealing their potential multifunctional applications in biomedical and environment fields.

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Acknowledgements

The authors extend their appreciation to UMM Al-Qura University, Saudi Arabia for funding this research work through grant number: 26UQU4350477GSSR05.

Funding

Declaration.

This research work was funded by UMM Al-Qura University, Saudi Arabia under grant number: 26UQU4350477GSSR05.

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Authors and Affiliations

  1. Department of Chemistry, Hazara University Mansehra, Mansehra, 21120, Pakistan

    Sadaf Ilyas Awan, Wajid Rehman & Rida Zameer

  2. Department of Chemistry, College of Science, Qassim University, Buraidah, 52571, Saudi Arabia

    Mona A. Alamri

  3. Chemistry Department, Faculty of Applied Science, Umm Al-Qura University, Makkah Almukkarramah, Saudi Arabia

    Thoraya A. Farghaly

  4. State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China

    Muhammed Shakeel

  5. Department of Chemistry, Faculty of Science, King Khalid University, Abha, 61413, Saudi Arabia

    Abdullah Y. A. Alzahrani

  6. Department of Microbiology, Hazara University Mansehra, Mansehra, 21120, Pakistan

    Farrukh Khan

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  1. Sadaf Ilyas Awan
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Correspondence to Wajid Rehman.

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Cite this article

Awan, S.I., Rehman, W., Zameer, R. et al. Synthesis and multi-technique structural characterization of trimetallic oxide nanocomposites for environmental and medicinal applications. Sci Rep (2026). https://doi.org/10.1038/s41598-026-49518-8

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  • Received: 06 February 2026

  • Accepted: 15 April 2026

  • Published: 30 April 2026

  • DOI: https://doi.org/10.1038/s41598-026-49518-8

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Keywords

  • Nanoparticles
  • Antibacterial
  • Antioxidant
  • Photocatalysis
  • Nanocomposites
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