Table 2 Data collection and refinement statistics.
| Â | Wild-type SOD1 | C57D/C146D mutant SOD1 |
|---|---|---|
Data collection | ||
Beamline | PAL 11 C | PAL 5 C |
Wavelength (Ã…) | 0.97942 | 0.97949 |
Space group | P32 | P21 |
Cell dimensions | ||
a, b, c (Ã…) | 112.430, 112.430, 209.280 | 49.319, 48.554, 55.015 |
α, β, γ (°) | 90, 90, 120 | 90, 93.17, 90 |
Resolution (Å) | 50.0–2.70 (2.75–2.70) | 50.0–1.80 (1.83–1.80) |
Rpim | 0.067 (0.157) | 0.045 (0.139) |
Rmerge | 0.167 (0.294) | 0.113 (0.297) |
I/σ | 8.3 (3.08) | 12.0 (3.8) |
Completeness (%) | 93.8 (78.9) | 96.7 (84.2) |
Redundancy | 4.9 (2.5) | 4.8 (3.3) |
Refinement | ||
Resolution (Å) | 49.52–2.7 | 36.38–1.80 |
No. reflections | 74868 | 21300 |
Rwork/Rfree | 0.2303/0.2473 | 0.1843/0.2130 |
No. total atoms | 14044 | 2363 |
Wilson B-factor (Ã…2) | 41.74 | 16.95 |
RMS deviations | ||
 Bond lengths (Å) | 0.001 | 0.008 |
 Bond angles (°) | 0.347 | 1.104 |
Ramachandran plot | ||
 Favored (%) | 94.40 | 98.95 |
 Allowed (%) | 5.44 | 1.05 |
 Outliers (%) | 0.16 | 0.0 |
PDB ID | 7FB9 | 7FB6 |
