Table 1 Crystallographic data collection and refinement statistics.

Space group

C 1 2 1

Cell dimensions

a, b, c (Å)

258.178, 69.373, 92.533

α, β, γ (°)

90, 109.68, 90

Resolution (Å)

121.55–3.24 (3.65–3.24)^a

R_merge

0.521 (1.395)

I / σI

3.2 (1.5)

Completeness (%)

63.2 (10.7)^b

Redundancy

6.6 (6.9)

Resolution (Å)

121.55–3.24 (3.65–3.24)

No. reflections

15692 (82)

R_work/R_free

0.282/0.290

No. atoms

9086

Protein

8974

Ligand/ion

112

Water

0

B-factors

Protein

48.88

Ligand/ion

42.35

R.m.s. deviations

Bond lengths (Å)

0.003

Bond angles (°)

0.519