Table 1 Crystallographic statistics of NopD-AtSUMO2 and NopD-Ubiquitin crystal structures

From: Broad-spectrum ubiquitin/ubiquitin-like deconjugation activity of the rhizobial effector NopD from Bradyrhizobium (sp. XS1150)

 

NopD-AtSUMO2

NopD-ubiquitin

Data collection

  Space group

P212121

P43

  Unit cell parameters (Å)

80.85, 86.83, 90.49

86.50, 86.50, 46.67

  Wavelength (nm)

0.9791

0.9792

  Resolution range (Å)

49.52–1.50

43.25–1.94

  Rmerge

0.07 (0.83)

0.07 (1.42)

  Rpim

0.03 (0.48)

0.03 (0.60)

  (I/σ(I))

14.2 (1.8)

13.3 (1.2)

  Completeness (%)

92.7 (48.9)

94.2 (55.0)

  Multiplicity

6.1 (3.7)

6.8 (6.6)

  CC (1/2)

0.99 (0.49)

0.99 (0.51)

Structure refinement

  Resolution range (Å)

49.52–1.50

43.25–1.94

  No. of unique reflections

76875

22770

  Rwork / Rfree (%)

17.84/20.36

17.16/19.94

  No. of atoms

    Protein

8363

2055

    Water molecules

312

62

  Overall B factors (Å2)

31.02

59.74

  Rms deviations

    Bonds (Å)

0.015

0.007

    Angles (°)

1.140

0.839

  Ramachandran favored (%)

99.22

98.41

  Ramachandran allowed (%)

0.59

1.19

  Ramachandran outliers (%)

0.2

0.4

PDB code

8OI3

8RQI

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