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Unequivocal identification of two-bond heteronuclear correlations in natural products at nanomole scale by i-HMBC

The inability to distinguish two-bond from long-range HMBC correlation has historically impeded NMR structure elucidation. Here the authors developed a practical iHMBC methodology utilizing accurate isotope shift measurement to overcome this limitation.

Yunyi Wang
Aili Fan
Xiao Wang
ResearchOpen Access03 Apr 2023
Nature Communications

Volume: 14, P: 1-11

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Unequivocal identification of two-bond heteronuclear correlations in natural products at nanomole scale by i-HMBC

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