Electrooxidation of biomass provides a sustainable route to produce valuable chemicals, but suffers from non-Faradaic degradation in alkaline electrolysis at high reactant concentration. Here, the authors develop a single-pass continuous flow reactor to tackle this challenge, achieving kilogram-scale and continuous electrooxidation of glucose to formate and 5-hydroxymethylfurfural to 2,5-furandicarboxylic acid with high selectivity and high concentration.
- Hua Zhou
- Yue Ren
- Haohong Duan