Table 1 Data collection and refinement statistics.
From: Molecular mechanism of strigolactone perception by DWARF14
D14 | D14−D-OH | |
|---|---|---|
Data collection* | ||
X-ray source | Photon Factory AR-NE3A | Rigaku FR-E rotating-anode X-ray generator |
Wavelength (Å) | 1.0000 | 1.5418 |
Space group | P212121 | P212121 |
Unit-cell parameters (Å) | a=48.1, b=88.7, c=118.6 | a=48.4, b=88.1, c=119.0 |
Resolution range (Å) | 20.0–1.75 (1.80–1.75) | 20.0–2.10 (2.15–2.10) |
No. of observed reflections | 37,0236 (20,889) | 215,098 (15,202) |
No. of unique reflections | 51,922 (3790) | 30,394 (2169) |
Average redundancy | 7.1 (5.5) | 7.1 (7.0) |
Completeness (%) | 99.8 (99.2) | 99.8 (100) |
Rsym | 0.076 (0.337) | 0.086 (0.430) |
Average I/σ(I) | 22.0 (6.5) | 20.4 (5.2) |
Refinement* | ||
Rwork/Rfree (%) | 18.3/22.3 | 19.1/24.6 |
No. of reflections | 49,279 | 28,858 |
No. of atoms | ||
Protein | 4074 | 4108 |
Ligand | − | 8 |
Water | 340 | 195 |
Mean B-value (Å2) | ||
Protein | 12.6 | 21.8 |
Ligand | − | 38.6 |
Water | 18.5 | 25.7 |
r.m.s.d. | ||
Bond lengths (Å) | 0.023 | 0.022 |
Bond angles (°) | 1.933 | 1.879 |
