Table 1 Data collection and refinement statistics.
From: The DUSP–Ubl domain of USP4 enhances its catalytic efficiency by promoting ubiquitin exchange
USP4 D1D2 | |
|---|---|
Data collection | |
Space group | P212121 |
Cell dimensions | |
a, b, c (Å) | 110.50, 151.03, 178.67 |
α, β, γ (°) | 90.0, 90.0, 90.0 |
Resolution (Å) | 44.6–2.4 (2.53–2.4) |
Rmerge (%) | 8.8 (66.1) |
I/σI | 11.0 (1.1) |
Completeness (%) | 94.9 (74.0) |
Redundancy | 3.4 (2.4) |
Refinement | |
Resolution (Å) | 44.6–2.4 (2.53–2.4) |
No. of reflections | 111,095 |
Rwork/Rfree | 17.8/21.0 |
No. of atoms | |
Protein | 15,884 |
Ligand/ion | 8 |
Water | 1,249 |
B-factors | |
Protein | 52.52 |
Ligand/ion* | 116.7 |
Water | 49.65 |
R.m.s.d. | |
Bond lengths (Å) | 0.010 |
Bond angles (°) | 1.02 |
