Table 11 Structural parameters of soot samples from XRPD

From: The reproduction of fire-born soot for comparative cleaning tests on heritage objects

Sample

Xc (%)

(002) peak

K = 0.89

(100) peak

K = 1.84

2ϑ (o)

FWHM

d002 (Å)

Lc (Å)

2ϑ (o)

FWHM

d100 (Å)

La (Å)

lamp black_NP

86.925

24.479

5.757

2.399

14.409

43.576

3.816

3.818

43.456

furnace black_Kr

85.157

24.364

5.525

2.055

15.338

43.558

3.803

3.661

43.685

carbon black_NP

81.585

24.350

5.318

2.019

15.981

43.750

3.518

6.647

46.480

candle soot

53.886

24 (LDCC)

6.810

1.436

13.671

/

 

26 (MDCC)

9.111

1.833

9.502

drum soot

51.662

24.650

5.231

3.223

15.466

/

  1. Thermal properties – TGA & EGA-MS.