Table 2 Data collection and refinement statistics
From: APOBEC3H structure reveals an unusual mechanism of interaction with duplex RNA
Nativea | Zn anomalousb | |
|---|---|---|
Data collection | ||
Space group | P22121 | P22121 |
Cell dimensions | ||
a, b, c (Å) | 88.0, 89.3, 134.4 | 90.4, 91.7, 139.3 |
α, β, γ (°) | 90, 90, 90 | 90, 90, 90 |
Wavelength (Å) | 1.033 | 1.283 |
Resolution (Å) | 44.6–2.24 (2.32–2.24) | 45.8–2.59 (2.68–2.59)c |
R merge | 0.128 (2.58) | 0.086 (1.08) |
R PIM | 0.03 (0.50) | 0.04 (0.45) |
R meas | 0.13 (2.63) | 0.09 (1.16) |
I/σI | 15.8 (1.09) | 15.7 (1.75) |
Completeness (%) | 1.00 (0.99) | 1.00 (0.99) |
Redundancy | 27.1 (26.4) | 7.1 (6.7) |
CC½ | 1 (0.48) | 1 (0.64) |
Refinement | ||
No. of reflections | 51,313 | |
R work/R free | 0.181/0.222 | |
No. of atoms | 7204 | |
Protein | 6120 | |
RNA | 830 | |
Zn | 4 | |
Water | 250 | |
Average B-factor (Å 2 ) | 84.4 | |
Protein | 85.3 | |
RNA | 79.5 | |
Zn | 78.2 | |
Water | 78.3 | |
R.m.s deviations | ||
Bond lengths (Å) | 0.002 | |
Bond angles (°) | 0.53 | |
