Table 1 Data collection and refinement statistics
From: A family of unconventional deubiquitinases with modular chain specificity determinants
ZUFSP S-SAD | ZUFSP native | |
|---|---|---|
Data collection | ||
Space group | P6522 | P6522 |
Unit cell constants | ||
a, b, c (Å) | 84.2, 84.2, 201.8 | 84.2, 84.2, 201.8 |
\(\alpha , \; \beta , \, \gamma\) (°) | 90, 90, 120 | 90, 90, 120 |
Wavelength (Å) | 2.07 | 0.98 |
Resolution (Å) | 59.13–2.3 (2.38–2.3) | 49.45–1.73 (1.79–1.73) |
No. of observations | 4,098,044 (364,012) | 484,411 (48,504) |
No. of unique reflections | 35,609 (3576)a | 44,866 (4337) |
Multiplicity | 115.1 (101.8) | 10.8 (11.2) |
Completeness (%) | 100 (100) | 100 (99) |
Rmerge (%) | 11.7 (39.5) | 8.4 (82.4) |
Rmeas (%) | 11.8 (39.7) | 14.3 (86.4) |
<I/\(\sigma\)(I)> | 47.7 (13.9) | 16.6 (2.5) |
CC1/2 (%) | 100 (99.7) | 99.8 (79.5) |
Anomalous signal | ||
CCano (59.13–3 Å [3.08–3.0 Å]) (%) | 56 (31) | |
Rpim (59.13– 3 Å [3.08–3.0 Å]) (%) | 0.8 (1.4) | |
Refinement | ||
Reflections used in refinement | 44,862 | |
Number of test reflections | 1930 | |
Rwork/Rfree (%) | 17.8/20.7 | |
Root-mean-square deviations | ||
Bond lengths (Å) | 0.005 | |
Bond angles (°) | 0.6 | |
Average B factor (Å2) | ||
All macromolecule atoms | 37.0 | |
Solvent molecules | 39.5 | |
Other atoms | 24.3 | |
Ramachandran plot (%) | ||
Most favored | 97.7 | |
Additionally allowed | 2.2 | |
Disallowed | 0.0 | |
