Table 1 Crystallographic data collection and refinement statistics
rSLFN1314–353 | rSLFN1314–353 | |
|---|---|---|
Data collection | ||
Data set | Native | SeMet derivative |
Space group | C2 | C2 |
Cell dimensions | ||
a, b, c (Å) | 172.05, 134.33, 77.66 | 171.96, 134.65, 77.69 |
α, β, γ (°) | 90, 105.51, 90 | 90, 104.72, 90 |
Wavelength (Å) | 0.97853 | 0.97931 |
Resolution (Å) | 50.0–3.18 (3.38–3.18)a | 50.0–3.50 (3.71–3.50) |
R sym | 0.049 (0.544) | 0.086 (0.525) |
I/σI | 17.08 (2.05) | 12.00 (2.81) |
Completeness (%) | 99.2 (98.4) | 99.4 (99.3) |
Redundancy | 3.41 (3.36) | 3.84 (3.87) |
Refinement | ||
Resolution (Å) | 35.24–3.18 (3.30–3.18) | |
No. reflections | 28,212 (2660) | |
Rwork/Rfree | 0.200/0.247 | |
Average B-factor | 108.67 | |
R.m.s. deviations | ||
Bond lengths (Å) | 0.003 | |
Bond angles (°) | 0.635 | |
Ramachandran plot (%) | ||
Favoured | 94.48 | |
Allowed | 4.97 | |
Outliers | 0.55 |