Table 1 Data collection and refinement statistics
From: Phase separation of Polo-like kinase 4 by autoactivation and clustering drives centriole biogenesis
CPB CP_v1 | CPB CP | |
|---|---|---|
Data collectiona | ||
Space group | P32 | P32 |
Cell dimensions | ||
a, b, c (Å) | 61.66, 61.66, 137.28 | 110.83, 110.83, 205.68 |
α, β, γ (°) | 90.00, 90.00, 120.00 | 90.00, 90.00, 120.00 |
Resolution (Å) | 50.0–2.64 (2.73–2.64) | 50.0–3.70 (3.83–3.70) |
Rmerge | 0.098 (1.093) | 0.159 (0.978) |
I /σI | 49.7 (2.8) | 23.75 (2.0) |
Completeness (%) | 99.9 (100.0) | 100.0 (100.0) |
Redundancy | 11.7 (11.6) | 11.0 (9.7) |
Refinement | ||
Resolution (Å) | 53.4–2.64 | 37.8–3.7 |
No. of reflections | 16,254 | 29,745 |
Rwork/Rfree | 0.2562/0.3131 | 0.2709/0.3092 |
No. of atoms | ||
Protein | 2940 | 14,008 |
Ligand/ion | 0 | 0 |
Water | 0 | 0 |
B factors | ||
Mean | 82.37 | 167.13 |
Max | 157.79 | 292.01 |
Min | 30 | 75. 95 |
R.m.s. deviations | ||
Bond lengths (Å) | 0.015 | 0.005 |
Bond angles (°) | 2.078 | 0.877 |
Ramachandran | ||
Favored | 91.00% | 97.84% |
Allowed | 99.23% | 99.94% |
Outliers | 0.77% | 0.06% |
