Table 1 Data collection and refinement statistics for X-ray crystallographic analysis of PTP1B_PS.

 Space group

P3₁21

   a, b, c (Å)

89.254, 89.254, 105.747

   α, β, γ (°)

90.000, 90.000, 120.000

 Resolution (Å)^a

52.87–1.89 (1.92–1.89)

 R_merge^a

0.071 (2.550)

 R_pim^a

0.025 (0.893)

 <I/σ(I)>^a

17.2 (1.1)

 CC_1/2^a

1.000 (0.626)

 Completeness (%)^a

100.0 (100.0)

 Multiplicity^a

9.0 (9.1)

 Resolution (Å)

44.67–1.89

 No. reflections

37270

 R_work /R_free

0.17922/0.21175

   Protein

2351

   Ligand/ion

1

   Water

224

   Protein^b

21.7

   Ligand/ion^b

50.8

   Water^b

47.4

   Bond lengths (Å)

0.008

   Bond angles (°)

1.488