Table. 1 Data collection and refinement statistics.
DslA form 1 | DslA form 2 | DslA E143Q | DslA E154Q | |
|---|---|---|---|---|
Accession code | 6TA9 | 6TAB | 6TAD | 6TAF |
Data collection | ||||
Space group | P21212 | P212121 | P212121 | P21212 |
Cell dimensions | 84.7, 47.8, 49.2 | 48.9, 64.7, 82.7 | 48.1, 62.1, 80.9 | 84.7, 47.9, 49.2 |
a, b, c (Å) α, β, γ (˚) | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 |
Resolution (Å) | 1.36 | 1.26 | 1.82 | 1.37 |
Rsym | 0.088 (0.785)a | 0.068 (1.786) | 0.161 (0.592) | 0.137 (1.713) |
Rpim | 0.026 (0.279) | 0.020 (0.696) | 0.022 (0.227) | 0.040 (0.489) |
I/σI | 16 (2) | 13 (1.2) | 20.1 (2.7) | 12.2 (2.2) |
CC½ | 0.998 (0.804) | 0.999 (0.509) | 0.998 (0.722) | 0.994 (0.617) |
Completeness (%) | 98.1 (82.8) | 99.8 (98.4) | 87.65 (21.1) | 98.4 (100) |
Redundancy | 12.4 (8.5) | 11.4 (7.5) | 49.5 (8.6) | 12.5 (13) |
Refinement | ||||
Rwork/Rfree | 14.0/18.0 | 15.0/17.7 | 17.2/21.0 | 17.7/19.5 |
R.m.s. deviations | ||||
Bond lengths (Å) | 0.006 | 0.014 | 0.006 | 0.005 |
Bond angles (°) | 1.03 | 1.55 | 0.79 | 1.04 |