Fig. 3: Scope of decarboxylative thiolation.
From: Manganese-mediated reductive functionalization of activated aliphatic acids and primary amines
Reaction conditions. aNHPI ester (0.3 mmol), disulfide (0.2 mmol), Mn (0.6 mmol), in DMA (0.2 M), 100 °C, N2, 15 h; yields are for isolated products. bNHPI ester (0.4 mmol). cWithout ligand. d1-Br was used. e1-I was used.
