Table 1 MAUS methyl resonance assignment statistics.

From: Backbone-independent NMR resonance assignments of methyl probes in large proteins

Target

MW (kDa)

PDB ID

Origin/resolution (Å)

Number of methyls

Labeling scheme

Short-range NOE distance

% Unique assignments

% Options ≤ 3 and >1

2ma

11.9

1JNJ

NMR

35

AILV

6.5

89

11

HLA-A01

45.5

6AT9

X-ray/2.9

87

AILV

7.2

64

30

HLA-A02

44.8

1DUZ

X-ray/1.8

94

AILV

6.0

70

15

MBP

40.7

1DMB

X-ray/1.8

76

MILVproS

6.0

75

21

IL-2

15.4

1M47

X-ray/1.9

61

ILV

6.5

74

23

HNHb

15.7

6O56

NMR/1.9

53

ILV

8.0

89

11

REC2

15.6

4CMP

X-ray/2.6

69

ILV

6.5

59

12

REC3

24.5

4ZT0

X-ray/2.9

85

ILV

8.0

67

28

  1. aNon-stereospecific.
  2. bUsed symmetrization and clustering tolerances of 0.1 ppm for 13C.