Fig. 5: Reductive coupling of various aryl halides.
From: Coupling photocatalytic water oxidation with reductive transformations of organic molecules
a Standard conditions: 0.5 mmol aryl halides, 15 mg Pd/g-C3N4* (2.8 wt% Pd), 1.5 equiv Na2CO3, 5 mL H2O, 3 mL 1,4-dioxane, argon atmosphere, 20 h, room temperature (25 oC), light source: 420 ± 10 nm LED (incident light intensity: 0.15 W/cm2), all the data shown in this figure are the isolated yields unless otherwise specified; b 10 h, GC yield; c incident light intensity: 0.10 W/cm2, GC yield; d 365 ± 10 nm LED; e 3 h, GC yield.
