Fig. 3: Functionalization of complex molecules via electrochemical halogen-atom transfer (e-XAT).

Reaction conditions: RVC anode, Pt cathode, alkyl iodides (0.3 mmol), CH₃CN (4.5 mL), H₂O (0.45 mL), N₂, 3.0 mA, 10 F/mol, 50 °C, 28 h. ^a48 h, 18 F/mol. Isolated yields.