Fig. 5: Scope of simple cyclic amine derivatives.
From: Electrochemical synthesis of peptide aldehydes via C‒N bond cleavage of cyclic amines
Reaction conditions: Undivided cell, graphite felt (GF) anode, platinum plate (Pt) cathode, 62a-76a (0.3 mmol), nBu4NPF6 (0.3 mmol), MeCN/H2O (9:1, 10 mL), constant current = 8.0 mA, 3 h (3.0 F), RT, under air. Isolated yields are reported. [a] 6.0 h. [b] Yield based on recovered starting materials.
